Study of the effect of substituents on the displacement of chemical shifts of N, N’-diarylureas in the nuclear magnetic resonance spectra

Views: 86 / PDF downloads: 64

Authors

A Bakibaev
M Sadvakassova
R Erkasov
A Sorvanov
A Аtagulova

DOI:

https://doi.org/10.32523/2616-6771-2020-131-2-18-22

Abstract

In our work, we studied the effect of substituents on chemical shifts in the nuclear magnetic resonance spectra.
The ranges of changes in chemical shifts From(1) to(10) carbon atoms, aromatic protons, carbonyl atoms, and urea protons in
diarylureas are considered. The analysis of N,N’-diarylureas by NMR 1 H and 13 C allows us to reliably identify the studied
compounds and serve as an additional method for quality control of pharmaceutical substances containing such drugs.

Downloads

Download data is not yet available.

Downloads

PDF (Русский)

Published

2022-12-29

Issue

Vol. 131 No. 2 (2020)

Section

Статьи

Most read articles by the same author(s)

О Ponomarenko, С Panshina 2, A Bakibaev, A Tashenov, Synthesis and identification of bicyclic bisurea esters , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 128 No. 3 (2019)
A Bakibaev, M Sadvakassova, R Erkasov, A Atagulova, Identification and analysis of N-arylalkyl-N’-acylureas by magnetic nuclear resonance , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 129 No. 4 (2019)
S Belykh , K Zhumanov, A Bakibaev, S Panshina, V Malkov, O Kotelnikov, L Tsoy, V Massalimova, Е Baibazarova, Salt synthesis of monoethanolamine with oxyethylenendiphosphonic acid , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 125 No. 4 (2018)
A Bakibaev, M Sadvakassova, R Erkasov, A Atagulova, Identification and analysis of N-alkyl-N’-arylalkylureas by nuclear magnetic resonance , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 130 No. 1 (2020)
A Belgibaeva, R Erkasov, I Kurzina, N Karakchieva, V Sachkov, Yu Abzaev, Receiving highly strong alloys of Ti-Al system by using metal hydride , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 126 No. 1 (2019)
G Baisalova, A Кoкоraевa, R Erkasov, D Amangeldy, Secondary metabolites of plants possessing antimicrobial and antibacterial activity against pathogens of brucellosis, pasteurellosis , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 126 No. 1 (2019)
A Belgibaeva, R Erkasov, I Kurzina, N Karakchieva, V Sachkov, Yu Abzaev, The effect of scandium micro alloying on the structure of alloys based on titanium aluminates , BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series: Vol. 131 No. 2 (2020)